Rotary Evaporators thiab lub tshuab nqus tsev distillation

Muaj qhov sib txawv tseem ceeb ntawm rotary evaporation apparatus thiab lub tshuab nqus tsev distillation zoo tib yam nyob rau hauv ntau yam, uas yog feem ntau cuam tshuam los ntawm lub hauv paus ntsiab lus, daim ntawv thov Scope, cov khoom muaj pes tsawg leeg thiab cov yam ntxwv ntawm kev ua haujlwm.

Rotary distillation:Rotary distillation yog hluav taws xob tswj los ua kom lub distillation flask tig ntawm qhov ceev ntawm qhov ceev tshaj plaws kom ua rau thaj tsam evaporation. Nyob rau tib lub sij hawm, lub tshuab nqus tsev twj tso kua mis ua rau lub evaporation flask nyob rau hauv lub tsis zoo siab lub xeev, txo lub boiling point ntawm cov tshuaj, thiab yog li accelerates lub evaporation ceev. Rotary steaming combines ob qho tib si kev sib hloov thiab decompression los txhim kho evaporation efficiency.

Ordinary nqus tsev distillation:Lub tshuab nqus tsev distillation (tseem hu ua lub tshuab nqus tsev distillation) feem ntau txo qhov kub ntawm cov kua los ntawm kev txo lub siab nyob rau hauv lub cev, kom tsis txhob muaj kev phiv tshuaj nyob rau hauv cov txheej txheem distillation ntawm high-boiling tshuaj los yog cov tebchaw uas yooj yim rau decompose, oxidize los yog polymerize thaum atmospheric distillation. Lub tshuab nqus tsev distillation feem ntau yog nyob ntawm lub tshuab nqus tsev distillation kom ua tiav kev sib cais thiab ua kom huv.

 

Rotary distillation:Teb distillation yog tsuas yog siv rau kev nruam distillation ntawm volatile solvents nyob rau hauv lub tshuab nqus tsev tej yam kev mob, dav siv nyob rau hauv chemistry, tshuaj kev lag luam, biomedicine thiab lwm yam teb. Vim nws txoj kev ua haujlwm siab thiab txuas ntxiv mus, rotary steaming yog tshwj xeeb tshaj yog haum rau kev tuav cov qauv loj lossis qhov yuav tsum tau tshem tawm cov kuab tshuaj sai.

Ordinary nqus tsev distillation:Nqus distillation yog tshwj xeeb tshaj yog haum rau kev sib cais thiab purification ntawm cov khoom uas muaj boiling ntsiab lus thiab cov tebchaw uas tau thermal decomposed, oxidized, los yog polymerized ua ntej mus txog boiling point nyob rau hauv atmospheric distillation. Cov tebchaw no nyuaj rau kev cuam tshuam nrog nyob rau hauv atmospheric siab, tab sis lawv cov ntsiab lus kub hnyiab tuaj yeem txo qis los ntawm lub tshuab nqus tsev distillation, kom lawv tuaj yeem sib cais thiab huv.

 

Rotary distillation:Rotary distillation khoom yog tsim los ntawm lub cev muaj zog, distillation fwj, cua sov lauj kaub, condensing raj thiab lwm yam. Lub raj mis distillation tig ntawm qhov ceev tsis tu ncua uas tau tsav los ntawm lub cev muaj zog, thaum lub lauj kaub cua sov muab cov cua sov tas li, thiab cov raj xa dej siv los sau cov kuab tshuaj evaporated.

General Vacuum Distillation:Lub tshuab nqus tsev distillation suav nrog peb ntu: distillation, rho tawm (nqus) thiab kev tiv thaiv thiab ntsuas ntsuas ntsuas nruab nrab ntawm lawv. Lub distillation ib feem muaj xws li lub raj mis distillation, lub taub hau Clarifier distillation, ib tug ncaj condensing raj, thiab lwm yam. Lub twj tso kua mis feem ntau yog siv lub twj tso kua mis, circulating dej nqus twj tso kua mis los yog lub tshuab nqus tsev twj tso kua mis kom tiav decompression; Kev tiv thaiv thiab ntsuas ntsuas cov cuab yeej siv los ua kom muaj kev nyab xeeb thiab raug ntawm qhov system.

 

Rotary distillation:Kev ua haujlwm rotary distillation yog qhov yooj yim, tuaj yeem ua tiav cov distillation tas li thiab tsis siv neeg sau cov kuab tshuaj. Los ntawm kev kho qhov kev sib hloov ceev thiab cua sov, cov txheej txheem distillation tuaj yeem tswj tau yooj yim thiab evaporation efficiency tuaj yeem txhim kho.

General Vacuum Distillation:Lub tshuab nqus tsev distillation ua haujlwm yog qhov nyuaj, xav tau kev tswj xyuas meej ntawm lub siab thiab kub hauv qhov system. Thaum lub sijhawm ua haujlwm, lub kaw lus nruj thiab siab ruaj khov yuav tsum tau kuaj xyuas tsis tu ncua kom ntseeg tau tias cov nyhuv distillation.

 

 

Qhov zoo thiab qhov tsis zoo ntawm rotary steaming

Qhov zoo:

Kev ua haujlwm zoo: Lub tshuab hluav taws xob sib txuas ua rau thaj tsam evaporation los ntawm lub tshuab hluav taws xob distillation thiab txo qhov system siab ua ke nrog lub tshuab nqus tsev twj, uas ua kom cov evaporation efficiency thiab ua rau cov qauv loj nyob rau hauv ib lub sij hawm luv luv los yog tshem tawm sai ntawm cov kuab tshuaj.

Yooj yim rau kev khiav lag luam: rotary steaming khoom feem ntau muaj kev tswj tsis siv neeg, tus neeg siv tuaj yeem teeb qhov kub thiab ceev tom qab cov txheej txheem evaporation tsis siv neeg, tsis muaj kev cuam tshuam ntau dhau.

Kev siv ntau yam: kev siv tshuaj tua kab mob tuaj yeem cuam tshuam nrog ntau yam sib txawv ntawm cov tshuaj, suav nrog cov kua qaub thiab alkaline thiab cov kuab tshuaj organic, muaj ntau yam kev siv.

Cov txiaj ntsig zoo concentration: evaporation ntawm lub tshuab nqus tsev ntau dua ua rau cov kua dej hauv cov tshuaj tau txais txiaj ntsig zoo dua concentration.

Qhov tsis zoo:

Cov cuab yeej siv siab: Tus nqi siab ntawm cov khoom siv evaporation piv rau lwm yam khoom siv evaporation tuaj yeem txwv nws daim ntawv thov hauv qee qhov kev sim qis lossis ntau lawm.

Lub peev xwm tuav tau tsawg kawg nkaus rau cov khoom siv hluav taws xob: qhov kub thiab txias uas tsim los ntawm cov txheej txheem spin steaming yuav ua rau cov khoom hloov pauv lossis poob ntawm cov khoom siv hluav taws xob.

Kev xaiv cov kuab tshuaj txwv tsis pub: Txawm hais tias teb distillation tuaj yeem daws ntau yam kev daws teeb meem, rau qee cov kuab tshuaj nrog ntau dua polarity, lawv cov evaporation efficiency yuav cuam tshuam.

 

Qhov zoo thiab qhov tsis zoo ntawm lub tshuab nqus tsev distillation

Qhov zoo:

Txo qhov kub hnyiab: Los ntawm kev txo lub siab nyob rau hauv lub cev, lub tshuab nqus tsev distillation zoo tib yam tuaj yeem txo qhov kub ntawm cov khoom, yog li ua tiav cov distillation ntawm qhov kub thiab txias, txo kev siv zog thiab tsis txhob decomposition lossis inactivation ntawm cov khoom los ntawm qhov kub thiab txias.

Txhim kho cov khoom purity: lub tshuab nqus tsev distillation tuaj yeem cais cov impurities, tshuaj lom thiab teeb meem thiab cov ntsiab lus qis hauv qhov sib tov, txhim kho purity thiab zoo ntawm cov khoom.

Kev siv dav: lub tshuab nqus tsev distillation yog siv dav hauv roj av, tshuaj, zaub mov thiab lwm yam lag luam, yog ib qho tseem ceeb ntawm kev sib cais tshuab.

Qhov tsis zoo:

Kev ua haujlwm nyuaj: Piv nrog cov cuab yeej siv tshuab ntau dua xws li cov tshuab hluav taws xob teb, kev ua haujlwm ntawm cov khoom siv tshuab nqus tsev zoo tib yam tuaj yeem ua haujlwm ntau dua, yuav tsum muaj kev tswj xyuas qhov siab thiab kub hauv qhov system.

Cov cuab yeej siv siab: lub tshuab nqus tsev distillation yuav tsum tau nruab nrog lub tshuab nqus tsev, uas muaj cov kev xav tau siab rau lub siab tsis kam ntawm lub thawv, ua rau qhov nyuaj thiab tus nqi ntawm cov khoom siv.

Kev tswj xyuas tsis yooj yim: cov cuab yeej siv tshuab nqus tsev distillation yuav tsum muaj kev tshuaj xyuas thiab kev saib xyuas tsis tu ncua los xyuas kom meej qhov nruj thiab kev ruaj ntseg ntawm lub cev, uas tuaj yeem ua rau muaj kev nyuaj siab thiab nqi kho.

 

 

Rotary evaporation thiab lub tshuab nqus tsev distillation yog tsim nyog rau ntau lub sijhawm thiab thaj chaw, raws li hauv qab no:

Daim ntawv thov thiab teb ntawm rotary evaporation (rotary evaporation)

Chemistry:

Distillation feem ntau yog siv los cais thiab mloog cov tshuaj tiv thaiv sib tov thaum lub sij hawm tshuaj synthesis thiab npaj. Los ntawm ob qho kev ua haujlwm ntawm kev sib hloov thiab decompression, cov kuab tshuaj tuaj yeem raug tshem tawm sai thiab ua tau zoo kom tau txais cov khoom xav tau los yog mloog zoo.

Pharmaceutical teb:

Nyob rau hauv cov txheej txheem tshuaj, rotary distillation tuaj yeem siv rau kev sib cais thiab kev ua kom huv, nrog rau kev sib xyaw ntawm cov tshuaj thiab cov nqa khoom. Nws tuaj yeem pab cov kws kho tshuaj txhim kho cov purity thiab zoo ntawm cov tshuaj thiab ua kom muaj kev nyab xeeb thiab ua tau zoo ntawm cov tshuaj.

Kev ua zaub mov:

Rotary distillation kuj tau siv dav hauv kev lag luam ua zaub mov rau kev sib xyaw, sib cais thiab rho tawm cov khoom noj lossis cov khoom noj ntxiv. Los ntawm rotary steaming, dej ntau dhau thiab impurities hauv cov zaub mov tuaj yeem raug tshem tawm, thiab qhov zoo thiab saj ntawm cov zaub mov tuaj yeem txhim kho.

Petrochemical teb:

Hauv kev lag luam petrochemical, rotary distillation tuaj yeem siv rau kev sib cais thiab cov ntsiab lus ntawm impurities xws li hydrogen sulfide thiab lwm yam roj av muaj kuab lom. Qhov no yuav pab txhim kho cov khoom siv roj av zoo thiab txo cov pa phem ib puag ncig.

Tshawb nrhiav thiab Laboratory:

Vim tias nws cov kev ua haujlwm siab thiab qib siab ntawm automation, cov khoom siv distillation rotary yog tshwj xeeb tshaj yog tsim rau kev tshawb fawb thiab kev sim hauv ib puag ncig. Cov kws tshawb fawb tuaj yeem siv cov cuab yeej siv hluav taws xob sib cais rau kev sib cais, kev ua kom huv thiab muaj zog ntawm ntau lub tebchaw los ua kom cov txheej txheem tshawb fawb thiab txhim kho qhov ua tau zoo ntawm qhov kev sim.

 

Daim ntawv thov thiab teb ntawm lub tshuab nqus tsev distillation

Kev sib cais ntawm cov ntsiab lus kub boiling:

Rau cov khoom uas muaj cov ntsiab lus kub siab dua, lub tshuab nqus tsev distillation zoo tib yam tuaj yeem ua tiav kev sib cais ntawm qhov kub thiab txias, tsis txhob decomposition lossis inactivation ntawm cov khoom uas yuav tshwm sim los ntawm qhov kub thiab txias.

Purification ntawm tshav kub-sensitive tshuaj:

Rau qee cov khoom kub-rhiab heev, lub tshuab nqus tsev zoo tib yam tuaj yeem ua tiav cov txheej txheem purification ntawm qhov kub thiab txias, txo qhov kev puas tsuaj ntawm cov khoom siv.

Petrochemical Kev Lag Luam:

Hauv kev lag luam petrochemical, lub tshuab nqus tsev distillation yog dav siv hauv roj fractionation, hnyav roj ua thiab lwm yam txheej txheem. Los ntawm lub tshuab nqus tsev distillation, cov khoom sib txawv hauv cov roj crude tuaj yeem sib cais raws li qhov sib txawv ntawm qhov kub thiab txias, thiab ntau yam khoom distillate tuaj yeem tau txais.

Kev lag luam zoo chemical:

Hauv kev lag luam tshuaj zoo, lub tshuab nqus tsev distillation kuj yog siv los cais thiab ntxuav ntau yam tshuaj zoo. Cov tshuaj no feem ntau muaj cov qauv nyuaj thiab cov khoom tshwj xeeb uas xav tau cov txheej txheem sib cais tshwj xeeb xws li lub tshuab nqus tsev distillation kom tau txais cov khoom zoo.

Pharmaceutical Industry:

Hauv kev lag luam kws tshuaj, lub tshuab nqus tsev distillation kuj tseem siv los npaj cov khoom siv tshuaj purity siab. Cov impurities thiab hnyav residues nyob rau hauv cov ntaub ntawv raw ntawm cov tshuaj yuav raug tshem tawm los ntawm lub tshuab nqus tsev distillation, thiab cov purity thiab zoo ntawm cov tshuaj yuav raug txhim kho.