Kev kub siab autoclave reactor
Aug 09, 2024
Tso lus
A Siab Siab Autoclave Reactoryog ib hom khoom siv uas muaj peev xwm ua cov tshuaj tiv thaiv nyob rau hauv qhov kub thiab txias. Nws yog dav siv nyob rau hauv chemistry, khoom siv science, biological engineering, kws tshuaj thiab lwm yam kev lag luam, rau synthesis, catalysis, hydrolysis, polymerization thiab lwm yam tshuaj tiv thaiv txheej txheem.

Basic qauv
Lub autoclave reactor yog tsim los ntawm lub cev reactor, cua sov system, stirring system, siab tswj system, kub tswj system thiab kev ruaj ntseg ntaus ntawv.
Lub cev Reactor:Feem ntau yog ua los ntawm stainless hlau (xws li SS 316) los yog tshwj xeeb alloys (xws li Hastelloy C / B, Monel, Inconel, Nickel, Titanium, Tantalum, thiab lwm yam) kom tiv taus qhov kub thiab txias ib puag ncig, thiab muaj corrosion kuj zoo.
Cua sov system:Los ntawm hluav taws xob cua sov, chav cua sov lossis roj da dej cua sov, thiab lwm yam, los muab cov thermal zog rau cov tshuaj tiv thaiv.
Stirring system:magnetic stirring los yog mechanical stirring method yog siv los xyuas kom meej tias cov reactants sib tov sib npaug hauv lub hwj thiab txhim kho cov tshuaj tiv thaiv.
Siab tswj qhov system:Los ntawm cov sensors siab thiab tsis siv neeg li qub thiab lwm yam khoom siv, kev saib xyuas lub sijhawm tiag tiag thiab kev tswj xyuas lub siab ntawm lub hwj kom paub meej tias cov tshuaj tiv thaiv tau ua nyob rau hauv qhov chaw nyab xeeb.
Kub tswj qhov system:Los ntawm qhov ntsuas kub thiab ntsuas ntsuas kub thiab lwm yam khoom siv, kev tswj xyuas meej ntawm cov tshuaj tiv thaiv kub kom ua tau raws li qhov xav tau ntawm cov kev xav sib txawv.
Khoom siv kev nyab xeeb:Xws li kev tiv thaiv overpressure, tiv thaiv overtemperature, kev kub ntxhov ceev thiab lwm yam khoom siv, kom ntseeg tau tias nyob rau hauv cov xwm txheej txawv txav tuaj yeem raug txiav tawm ntawm lub sijhawm hluav taws xob, txo qhov siab lossis kub, kom ntseeg tau tias muaj kev nyab xeeb ntawm cov khoom siv thiab cov neeg ua haujlwm.
Txoj cai ua haujlwm

Lub hauv paus ntsiab lus ntawm kev ua haujlwm ntawm autoclave reactor yog muab cov reactants rau hauv lub reactor, thiab muab lub zog cua sov los ntawm cov cua sov, kom cov reactants tuaj yeem ua cov tshuaj tiv thaiv nyob rau hauv qhov kub thiab txias.
Nyob rau tib lub sijhawm, cov txheej txheem nplawm kom ntseeg tau tias cov reactants sib npaug sib xyaw hauv lub reactor, txhim kho cov tshuaj tiv thaiv.
Thaum lub sij hawm cov txheej txheem cov tshuaj tiv thaiv, lub siab tswj qhov system thiab kub tswj system saib xyuas thiab tswj lub siab thiab kub nyob rau hauv lub hwj nyob rau hauv lub sij hawm ntawm lub sij hawm los xyuas kom meej tias cov tshuaj tiv thaiv yog nqa tawm nyob rau hauv kev nyab xeeb thiab ruaj khov.
Kev ua haujlwm
Kev ua haujlwm ntawm lub siab kub siab autoclave reactor muaj ob peb kauj ruam, los ntawm kev npaj cov reactants thiab thauj mus rau hauv lub reactor nkoj mus saib xyuas cov tshuaj tiv thaiv thiab sau cov khoom.
◆ Kev npaj
Ua ntej thauj cov reactants rau hauv lub nkoj reactor, nws yog ib qho tseem ceeb uas yuav tsum tau ua tib zoo ntsuas thiab sib tov rau hauv qhov tsim nyog proportions. Txhua yam impurities lossis cov khoom paug hauv cov reactants tuaj yeem cuam tshuam qhov tshwm sim ntawm cov tshuaj tiv thaiv.
◆ Chaw thau khoom
Tom qab ntawd cov reactants raug thauj mus rau hauv lub nkoj reactor, uas feem ntau raug kaw nrog lub hau gasketed lossis flange. Kev saib xyuas tshwj xeeb yuav tsum tau ua kom ntseeg tau tias lub nkoj tau raug kaw kom zoo kom tsis txhob xau thaum cov tshuaj tiv thaiv.
◆ Kev kub siab thiab cua sov
Thaum cov reactants tau loaded, lub nkoj reactor yog pressurized mus rau qib uas xav tau siv ib tug inert gas xws li nitrogen los yog helium. Tom qab ntawd lub tshuab cua sov yog qhib, thiab qhov kub hauv lub nkoj tau maj mam nce mus rau qhov xav tau.
◆ Kev saib xyuas
Thoob plaws hauv cov tshuaj tiv thaiv, tus neeg teb xov tooj yuav tsum ua tib zoo saib xyuas lub siab thiab kub hauv lub reactor hlab ntsha. Kev hloov kho yuav tsim nyog los tswj cov kev xav tau, thiab cov tshuaj tiv thaiv sib xyaw yuav tsum tau nplawm ib ntus kom ntseeg tau tias sib xyaw ua ke.
◆ Sau
Tom qab cov tshuaj tiv thaiv tiav, lub nkoj reactor txias thiab depressurized. Tom qab ntawd cov khoom raug sau thiab tshuaj xyuas los txiav txim siab lawv cov muaj pes tsawg leeg thiab purity.
Kev tsim kho thiab khoom siv
Kev kub siab autoclave reactors yog tsim los nrog cov ntaub ntawv uas tuaj yeem tiv taus qhov kub thiab txias. Feem ntau, lub cev reactor yog ua los ntawm cov ntaub ntawv xws li ntshiab titanium (TAI-2), Hastelloy C-207, los yog 316L stainless hlau. Cov ntaub ntawv no muaj zoo heev corrosion kuj thiab txhua yam muaj zog, ua kom lub reactor lub durability thiab ntev. Lub rooj ua haujlwm, ntawm qhov tod tes, feem ntau yog ua los ntawm 316L stainless hlau kom yooj yim tu thiab tu.
Lub reactor yog tsim los tiv taus siab txog li 6 MPa thiab kub hauv qab 400 degree. Lub tshuab cua sov, feem ntau suav nrog lub tshuab hluav taws xob hluav taws xob lossis lub nplhaib hluav taws xob, muab kev tswj kub ceev thiab meej nrog lub zog cua sov xws li 300W txog 500W. Kev tswj qhov kub thiab txias yog qhov tseeb heev, nrog rau qhov tseeb ntawm ± 1 degree, kom ntseeg tau tias cov tshuaj tiv thaiv cov xwm txheej raug tswj xyuas nyob rau hauv cov npoo nruj.
Lub reactor tseem muaj ntau yam li qub thiab fittings, ntau yam uas tau los ntawm lub teb chaws Yelemees, kom ntseeg tau tias kev ua haujlwm tsis zoo thiab kev sib raug zoo nrog ntau yam kev sim teeb tsa. Lub tshuab nplawm, uas yog ib qho tseem ceeb rau kev ua tiav homogeneous cov tshuaj tiv thaiv sib tov, yog digitally tswj thiab tuaj yeem ncav cuag qhov nrawm mus txog 1500 RPM nrog qhov tseeb ntawm 3-5 RPM.
Daim ntawv thov
Kev kub siab autoclave reactors muaj ntau yam kev siv hauv kev tshawb fawb thiab kev lag luam. Qee qhov kev siv ntau tshaj plaws suav nrog:
Cov tshuaj tiv thaiv catalytic:Lub tshuab hluav taws xob muaj peev xwm tswj tau qhov kub thiab txias thiab lub zog siab ua rau nws zoo tagnrho rau kev kawm thiab ua kom zoo dua cov tshuaj tiv thaiv catalytic. Cov kws tshawb fawb tuaj yeem siv nws los tshawb xyuas qhov cuam tshuam ntawm cov catalysts sib txawv, reactant concentrations, thiab cov kev mob tshwm sim ntawm cov tshuaj tiv thaiv tus nqi thiab cov khoom faib khoom.
High-temperature thiab high-pressure synthesis:Lub reactor tuaj yeem siv los tsim cov tebchaw uas xav tau qhov kub thiab txias rau lawv qhov tsim. Qhov no suav nrog kev sib txuas ntawm cov ntaub ntawv tsis muaj organic, polymers, thiab organometallic compounds.
Kinetics kev tshawb fawb:Los ntawm kev saib xyuas cov kev mob tshwm sim hauv lub sijhawm tiag tiag, cov kws tshawb fawb tuaj yeem siv lub reactor los kawm txog kinetics ntawm ntau yam tshuaj tiv thaiv, nrog rau tus nqi ntawm cov tshuaj tiv thaiv, ua kom lub zog, thiab cov tshuaj tiv thaiv mechanism.
Cov tshuaj tiv thaiv tshwj xeeb:Lub reactor kuj tseem siv rau cov tshuaj tiv thaiv tshwj xeeb xws li Fischer-Tropsch synthesis, hydrogenation reactions, thiab polymerizations.
Kev Txawj Ntse
Kev nce qib tsis ntev los no hauv kev kub siab autoclave reactor thev naus laus zis tau ua rau lawv muaj ntau yam thiab siv tau zoo. Piv txwv li, qee lub reactors tam sim no muaj RS232 kev sib txuas lus sib txuas uas tso cai rau lawv txuas nrog cov khoos phis tawj rau kev nrhiav cov ntaub ntawv thiab tshuaj xyuas. Qhov no ua rau cov kws tshawb fawb los saib xyuas thiab tswj cov tshuaj tiv thaiv nyob deb thiab khaws thiab txheeb xyuas cov ntaub ntawv sim tau zoo dua.
Tsis tas li ntawd, kev txhim kho ntawm ntau lub tshuab hluav taws xob tau ua rau nws muaj peev xwm ua kom muaj kev sib txuam sib luag nyob rau hauv cov xwm txheej sib txawv lossis ua raws li cov kev xav hauv tib lub reactor. Qhov no tsis tsuas yog txuag lub sijhawm thiab cov peev txheej xwb tab sis kuj tso cai rau cov kws tshawb fawb los txhim kho cov xwm txheej tshwm sim ntau dua.


